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Labsolar-IIIAG On-line photocatalytic analysis system

Labsolar-IIIAG 在线光催化分析系统

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Labsolar-IIIAG Online Photocatalytic Analysis System with an all-glass construction, fundamentally eliminating errors caused by metal adsorption on experimental results; magnetic circulation air pump with no electrical connections in the system, eliminati
  • Introduction
  • Application
  • Literature
  • Maintenance

Key Features

● Classic structural design with numerous satisfied customers, offering exceptional cost-effectiveness;

● All-glass material construction, fundamentally preventing errors caused by metal adsorption on experimental results;

● Dual seven-way sampling structure to eliminate carrier gas mis-sampling;

● Magnetic circulation air pump with no electrical connections in the system, eliminating the risk of hydrogen explosions and interference from electrolysis hydrogen generation.

 

Application Fields

▲ Especially suitable    ● Moderately suitable  ○ Can be used

▲ Photocatalytic/Photoelectrocatalytic hydrogen/oxygen production from water;

▲ Photocatalytic/Photoelectrocatalytic complete water decomposition;

▲ Photocatalytic/Photoelectrocatalytic CO₂ reduction;

▲ Photocatalytic quantum efficiency measurement.

 

Gas Circulation Parameters

● Linear standard curve: R² > 0.999 when H₂ content is in the range of 100 µL to 10 mL;

● Reproducibility: RSD < 3% when the same concentration is sampled four times in a row;

● Passive magnetic high-speed circulation system: Drive speed not less than 4000 r/min, with powerful circulation dynamics; no electrical connections in the pipeline, no risk of hydrogen explosion, and no interference from electrolysis hydrogen generation;

● Sampling method: Manual online sampling with multiple quantitative ring multi-port sampling valves made of high borosilicate glass, located in the system rather than the chromatograph;

● Circulation pipeline: The narrowest pipeline has an inner diameter of 3 mm, not a small-caliber chromatographic pipeline, with low gas resistance.

System Pipeline Parameters

● Absolute vacuum degree: ≤0.1 MPa;

● Range of use pressure: 0 kPa~atmospheric pressure;

● Gas tightness: Relative pressure change ≤1 kPa/24 h;

● Pipeline material: High borosilicate glass, high chemical inertness, no adsorption;

● Valve process: High borosilicate glass material, valve plug and valve sleeve using precision grinding process;

● Number of valves: 13;

● Vacuum grease: Imported Dow Corning vacuum grease, corrosion-resistant, low vapor pressure, low volatility, working temperature: -40°C~200°C;

● Pipeline volume: 150 mL;

● Quantitative ring: 1.5 mL;

● Gas storage bottle: 250 mL, suitable for system expansion and storage of reaction gases such as carbon dioxide;

● Condenser tube: Spherical condenser tube, preventing water vapor from entering the gas chromatograph and vacuum pump;

● Cold trap: Separation of low-boiling-point components, extending the life of the vacuum pump and improving system vacuum.

Exterior Structure and Other Accessories

● Reactor: Suitable for photocatalytic reactors and photoelectrocatalytic reactors; can be customized based on actual experimental needs;

● Overall size/mm: 650 (L) × 370 (W) × 730 (H);

● Open design: Highly adjustable according to experimental requirements;

● Optoelectronic isolation: Both input and output parts have optoelectronic isolation with strong anti-interference capability;

● Vacuum pump: Single-stage rotary vane vacuum pump, pumping speed ≥6L/s;

 

Representative References

Dalian Institute of Chemical Physics Academician Li Can's team cited Labsolar-IIIAG Photocatalytic Reaction System

Harbin Institute of Technology Professor Chen Gang's team cited IIIAG System

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